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A high-pressure single-crystal X-ray diffraction study of potassium guaninate hydrate, K+·C5H4N5O-·H2O. / Gaydamaka, Anna A; Rashchenko, Sergey V; Semerikova, Anna I et al.

In: Acta crystallographica Section B, Structural science, crystal engineering and materials, Vol. 79, No. Pt 6, 01.12.2023, p. 495-509.

Research output: Contribution to journal › Article › peer-review

Harvard

Gaydamaka, AA, Rashchenko, SV, Semerikova, AI, Smirnova, ES, Ivanova, AG, Arkhipov, SG, Zakharov, BA, Bogdanov, NE & Boldyreva, EV 2023, 'A high-pressure single-crystal X-ray diffraction study of potassium guaninate hydrate, K+·C5H4N5O-·H2O', Acta crystallographica Section B, Structural science, crystal engineering and materials, vol. 79, no. Pt 6, pp. 495-509. https://doi.org/10.1107/S2052520623008740

APA

Gaydamaka, A. A., Rashchenko, S. V., Semerikova, A. I., Smirnova, E. S., Ivanova, A. G., Arkhipov, S. G., Zakharov, B. A., Bogdanov, N. E., & Boldyreva, E. V. (2023). A high-pressure single-crystal X-ray diffraction study of potassium guaninate hydrate, K+·C5H4N5O-·H2O. Acta crystallographica Section B, Structural science, crystal engineering and materials, 79(Pt 6), 495-509. https://doi.org/10.1107/S2052520623008740

Vancouver

Gaydamaka AA, Rashchenko SV, Semerikova AI, Smirnova ES, Ivanova AG, Arkhipov SG et al. A high-pressure single-crystal X-ray diffraction study of potassium guaninate hydrate, K+·C5H4N5O-·H2O. Acta crystallographica Section B, Structural science, crystal engineering and materials. 2023 Dec 1;79(Pt 6):495-509. Epub 2023 Dec 1. doi: 10.1107/S2052520623008740

Author

Gaydamaka, Anna A ; Rashchenko, Sergey V ; Semerikova, Anna I et al. / A high-pressure single-crystal X-ray diffraction study of potassium guaninate hydrate, K+·C5H4N5O-·H2O. In: Acta crystallographica Section B, Structural science, crystal engineering and materials. 2023 ; Vol. 79, No. Pt 6. pp. 495-509.

BibTeX

@article{b7df50228e124d8cb153a7033ab92fa7,
title = "A high-pressure single-crystal X-ray diffraction study of potassium guaninate hydrate, K+·C5H4N5O-·H2O",
abstract = "The crystal structure of potassium guaninate hydrate, K+·C5H4N5O-·H2O, was studied in the pressure range of 1 atm to 7.3 GPa by single-crystal diffraction using synchrotron radiation and a laboratory X-ray diffraction source. Structural strain was compared to that of the same salt hydrate on cooling, and in 2Na+·C5H3N5O2-·7H2O under hydrostatic compression and on cooling. A polymorphic transition into a new, incommensurately modulated, phase was observed at ∼4-5 GPa. The transition was reversible with a hysteresis: the satellite reflections disappeared on decompression to ∼1.4 GPa.",
author = "Gaydamaka, {Anna A} and Rashchenko, {Sergey V} and Semerikova, {Anna I} and Smirnova, {Ekaterina S} and Ivanova, {Anna G} and Arkhipov, {Sergey G} and Zakharov, {Boris A} and Bogdanov, {Nikita E} and Boldyreva, {Elena V}",
year = "2023",
month = dec,
day = "1",
doi = "10.1107/S2052520623008740",
language = "English",
volume = "79",
pages = "495--509",
journal = "Acta Crystallographica Section B: Structural Science, Crystal Engineering and Materials",
issn = "2052-5192",
publisher = "Wiley-Blackwell",
number = "Pt 6",

}

RIS

TY - JOUR

T1 - A high-pressure single-crystal X-ray diffraction study of potassium guaninate hydrate, K+·C5H4N5O-·H2O

AU - Gaydamaka, Anna A

AU - Rashchenko, Sergey V

AU - Semerikova, Anna I

AU - Smirnova, Ekaterina S

AU - Ivanova, Anna G

AU - Arkhipov, Sergey G

AU - Zakharov, Boris A

AU - Bogdanov, Nikita E

AU - Boldyreva, Elena V

PY - 2023/12/1

Y1 - 2023/12/1

N2 - The crystal structure of potassium guaninate hydrate, K+·C5H4N5O-·H2O, was studied in the pressure range of 1 atm to 7.3 GPa by single-crystal diffraction using synchrotron radiation and a laboratory X-ray diffraction source. Structural strain was compared to that of the same salt hydrate on cooling, and in 2Na+·C5H3N5O2-·7H2O under hydrostatic compression and on cooling. A polymorphic transition into a new, incommensurately modulated, phase was observed at ∼4-5 GPa. The transition was reversible with a hysteresis: the satellite reflections disappeared on decompression to ∼1.4 GPa.

AB - The crystal structure of potassium guaninate hydrate, K+·C5H4N5O-·H2O, was studied in the pressure range of 1 atm to 7.3 GPa by single-crystal diffraction using synchrotron radiation and a laboratory X-ray diffraction source. Structural strain was compared to that of the same salt hydrate on cooling, and in 2Na+·C5H3N5O2-·7H2O under hydrostatic compression and on cooling. A polymorphic transition into a new, incommensurately modulated, phase was observed at ∼4-5 GPa. The transition was reversible with a hysteresis: the satellite reflections disappeared on decompression to ∼1.4 GPa.

UR - https://www.scopus.com/record/display.uri?eid=2-s2.0-85179885639&origin=inward&txGid=c7814e60f78b2a3fb094791f5ebc9cae

UR - https://www.mendeley.com/catalogue/a297b977-91f4-3ab3-bce8-cf347f411952/

U2 - 10.1107/S2052520623008740

DO - 10.1107/S2052520623008740

M3 - Article

C2 - 37934491

VL - 79

SP - 495

EP - 509

JO - Acta Crystallographica Section B: Structural Science, Crystal Engineering and Materials

JF - Acta Crystallographica Section B: Structural Science, Crystal Engineering and Materials

SN - 2052-5192

IS - Pt 6

ER -

ID: 57539056